The scatter slit should be at least as large as the widest opening of the
ADS - for the situation described above you should be using a 4deg scatter
slit.
There is a good discussion of the issues in :-
Bowden M.E. and Ryan M.J. (1991) Powder Diffraction, 6(2), 78-81.
Cheers
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Ian Madsen
CSIRO Minerals
Box 312
Clayton South 3169
Victoria
AUSTRALIA
Phone +61 3 9545 8785 direct
+61 3 9545 8500 switch
FAX +61 3 9562 8919
Email Ian.Madsen@minerals.csiro.au
XRD laboratory 'tour' starts at
http://www.minerals.csiro.au/public/work/res_equip/tour/begin.htm
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