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RE: [sdpd] Comparision of the intensities
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<p>First, I am assuming that preferred orientation is not an issue.<br>
<br>
Most zeolites are quite sensitive to the amount of bound water which can<br>
vary significantly with synthesis method and ambient humidity. The<br>
framework structure will be essentially the same but variation in water<br>
population in the cages will cause intensity variations especially in<br>
the low angle regions. <br>
<br>
Differences in the crystallite size will not cause a variation in the<br>
intensity distribution (area under the profile) or d-spacing. You may<br>
be able to figure out the cause of the intensity variation from a<br>
difference Fourier map. <br>
<br>
Dipo Omotoso<br>
<br>
____________<wbr>_________<wbr>_________<wbr>__<br>
<br>
From: <a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.<wbr>com</a> [mailto:<a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.<wbr>com</a>] On Behalf Of<br>
PRADEEP J. RAI<br>
Sent: September 22, 2008 1:25 AM<br>
To: <a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.<wbr>com</a><br>
Subject: [sdpd] Comparision of the intensities<br>
<br>
Dear all,<br>
<br>
I am facing problem in evaluating my zeolite material<br>
<br>
My synthesized zeolite tends to have the same d values as that of the <br>
standard but the intensity does not match. I have tried to match my 50 <br>
synthesis batch but standard seems to have higher intensity<br>
<br>
can any body suggest what is happening?<br>
has it anything to do with crystallite size.<br>
<br>
Looking forward to suggestion and comments.<br>
<br>
[Non-text portions of this message have been removed]<br>
<br>
</p>
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