Re: [sdpd] Hump ???

[Armel Le Bail <alb...@cristal.org>]

Hi,

The mystery is now evenmore thick... I recorded a
new pattern this night, without sample, and it is
confirmed that the single-humped camel (with sample)
tranformed into a nice double-humped camel (without
sample), periodical, d=4.4A...

See the figure :
http://www.cristal.org/empty2.jpg

See the D8 Advance mounting :
without sample, without holder
http://www.cristal.org/nosample1.jpg
wiithout sample, with empty holder
http://www.cristal.org/nosample2.jpg
The pattern with the Al2O2 NIST 1976 is
obtained by just inserting the AL2O3 plate
in the holder seen on the previous picture,
and the second hump close to 40° disappears...

Suggestions ?

Armel

PS - From my trip in Egypt in december 2004
for the ESCA-9 workshop, hump confirmation :
http://www.cristal.org/egypt-2004/13.jpg



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