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Re:[sdpd] How to quantify an amorphous phase in a multiphses sample by Rietveld refinement
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- Subject: Re:[sdpd] How to quantify an amorphous phase in a multiphses sample by Rietveld refinement
- From: 徐君 <xujun16...@163.com>
- Date: Sun, 11 Dec 2011 09:29:36 +0800 (CST)
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<p>Hi,<br>
<br>
>show me the details if this can be finished without an internal standard?<br>
First, if you do not know what the amorphous phase is, you have to be use the standard sample. Second, if the chemical composition of the amorphous, or as an alternative, of the whole sample is known, the standard cannot be added to the sample. <br>
<br>
If want to know how to do, please refer to QUANTO, GSAS, MAUD etc.<br>
<br>
Best regards,<br>
Xu Jun<br>
<br>
At 2011-12-10 19:00:32,daxuliu <<a href="mailto:daxuliu%40yahoo.com">daxuliu...@yahoo.com</a>> wrote:<br>
<br>
<br>
Hi, dear all,<br>
<br>
My question is how to get the amorphous phase weight% by Fullprof or other softs if no standard sample isn't added.<br>
For example, how do you get the exact weight% of the glass in sample 3 of IUCr CPD Round Robin on Quantitative Phase Analysis (<a href="http://www.iucr.org/resources/commissions/powder-diffraction/projects/qarr">http://www.iucr.org/resources/commissions/powder-diffraction/projects/qarr</a>)?<br>
Please show me the details if this can be finished without an internal standard. Thanks very much!<br>
<br>
sincerely daxu.<br>
<br>
[Non-text portions of this message have been removed]<br>
<br>
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