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Re: [sdpd] Re: DDM program update 1.92
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<p><br>
>The main problems of your data are an ugly peak asymmetry and <br>
>displacements due to, I suspect, a French wine you applied before <br>
>the measurements. I use Russian vodka that gives much more <br>
>symmetrical peaks and minimal displacements. Here, I'm afraid, I <br>
>disclosed the sacred Russian know-how, but I will burn in hell anyway...<br>
<br>
Continuing in explaining the whole Universe (including powder diffraction)<br>
with alcool vapor effecs :<br>
<br>
Asymmetry on the old Siemens D500 diffractemeter could be due essentially<br>
to the Siemens engineers, were they German ? Then, schnaps rather than wine<br>
or vodka ?<br>
<br>
About the sample displacement, it is observed frequently when attempts are made<br>
to avoid preferred orientation, then the sample is not pressed on its <br>
holder (Bragg Brentano)<br>
bur dusted through a sieve on the holder. In such conditions, it is <br>
difficult to have the<br>
sample exactly in the diffracting plane, it is generally above and <br>
loosely packed. French<br>
wine may have some benefit effect on the way to dust the sample with <br>
a perfect shaking<br>
hands. No doubt that such a shaking hand can be experienced too with <br>
vodka or schnaps.<br>
<br>
If others want to disclosed their secret know-how, there is room here.<br>
<br>
Best<br>
<br>
Armel<br>
<br>
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