Re: [sdpd] identifying the phase (amorphous to crystallize)

[Jonathan Wright <wright...@esrf.fr>]

Hi Armel, AI,

The ID11 staff are always interested! We would normally expect that some 
other spectra have been processed without problems? Assuming the 
difficulty is not related to data reduction or calibrations then the 
problem sounds crystallographic. With a mixed phase inter-metallic 
sample produced in-situ... I would just hope that it does not turn out 
to be incommensurate.

All the best,

Jon


Armel Le Bail wrote:
> 
> 
> Well, no one interested at the ID11 staff ?!
> 
> Send me the data...
> 
> Armel
> 
> At 14:17 28/05/2008 +0200, you wrote:
>  >Dear All,
>  >
>  >I am a very beginner in this field
>  >
>  >I have some spectras of bulk metallic glass taken from ESRF ID11. the
>  >spectra was taken as in situ experiment, sample is MgCuGd bulk metallic
>  >glass heated untill fully crystallize. I could not identify the phase 
> inside
>  >the fully crystallize spectra (it must be multiphase). I have use some
>  >databases (search match the spectra) that exist but still no good 
> solution.
>  >Phases like Mg2Cu, Cu2Mg may appears but could 90% justified. the main
>  >problem is my intensity is very very huge, there are many missing and
>  >shifted peaks. I use MAUD also for the quantitative analysis. Does anybody
>  >could give suggestion ?
>  >
>  >regards
>  >AI
>  >
>  >

------------------------------------

Yahoo! Groups Links

<*> To visit your group on the web, go to:
    http://groups.yahoo.com/group/sdpd/

<*> Your email settings:
    Individual Email | Traditional

<*> To change settings online go to:
    http://groups.yahoo.com/group/sdpd/join
    (Yahoo! ID required)

<*> To change settings via email:
    mailto:sdpd-digest...@yahoogroups.com 
    mailto:sdpd-fullfeatured...@yahoogroups.com

<*> To unsubscribe from this group, send an email to:
    sdpd-unsubscribe...@yahoogroups.com

<*> Your use of Yahoo! Groups is subject to:
    http://docs.yahoo.com/info/terms/