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Re: [sdpd] XRD intensity
Dear all
Thank you for the valuable suggestions. Anyway am still at loss in
increasing the intensity. Thank you for your kind support
>
>
> With this thin a film, and assuming it is polycrystalline, a theta-2theta
> geometry will give low intensities. You might be better off using a
> grazing incidence and scanning only the detector.
>
> Cheers,
>
> Carlo
>
> On Fri, 11 Mar 2005, Thierry Bataille wrote:
>
> >
> > Hysen
> > what is your diffractometer configuration ? Take care of fluorescence
> > arising from Fe in case of using for instance CuKa1 with a incident-beam
> > monochromator. Have you tried with a graphite monoch. behind your sample ?
> > Thierry
> >
> >
> > At 03:21 11/03/2005 +0000, vous avez écrit:
> >
> >
> >> Dear all
> >> I am hysen from cochin university ,Kerala. I am working on
> >> nanomagnetic materials. specifically an alloy of irom molybdenum boron
> >> and nickel. I have prepared thin films of this having thickness around
> >> 30 nm by resistive heating and annealed the sample upto the
> >> crystallization temperature of the bulk. But interestingly the xrd
> >> spectrum shows peaks which are very feeble which has intensity
> >> comparable to that of the noise. Can anybody has any suggestionsto
> >> improve the xrd spectrum. Due to this low intensity i cant do any fitting.
> >> Thank you in advance
> >> Hysen Thomas researcher
> >> Cusat
> >> Cochin 22
> >> Kerala
> >>
> >>
> >>
> >>
> >>
> >>
> >>
> >> Yahoo! Groups Links
> >>
> >>
> >>
> >>
> >>
> >
> > Thierry Bataille
> > LCSIM UMR CNRS 6511
> > Cristallographie des Poudres et Réactivité des Solides
> > Institut de Chimie de Rennes
> > Université de RENNES I
> > Avenue du Général Leclerc
> > F-35042 RENNES cedex, France
> >
> > Tel. (+33) 2 23 23 58 05 Fax. (+33) 2 23 23 68 40
> > mailto:Thierry.Bataille...@univ-rennes1.fr
> >
> > http://perso.univ-rennes1.fr/thierry.bataille
> >
> > http://www.lcsim.univ-rennes1.fr
> > http://www.chimie.univ-rennes1.fr
> >
> >
> >
> >
> >
> > Yahoo! Groups Links
> >
> >
> >
> >
> >
> >
> >
> >
>
> --
> Carlo U. Segre -- Professor of Physics
> Associate Dean for Special Projects, Graduate College
> Illinois Institute of Technology
> Voice: 312.567.3498 Fax: 312.567.3494
> Carlo.Segre...@iit.edu http://www.iit.edu/~segre
>
> [Non-text portions of this message have been removed]
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> Yahoo! Groups Links
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--
Hysen Thomas
Research Scholar
Department of Physics
Cochin University
Cochin22, Kerala
India
Visit www.cusat.ac.in/dop/maglab
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