Run PowderX. Select "File", "Import Data" and the format corresponding to your data (here Siemens *.uxd):
Ckick, and this will open a window. Search for your file,
select it and open it. The pattern should be drawn :
Click on the "subtract background" button, a box appears which proposes default values :
You may click on "Show" and the estimated background will be drawn. Using the zoom option, you may look at it and decide if you are satisfied (if not, play on the "pickup point" and "repeating time") :
Note that you have to close the zoom window and open it again at each test. Well, you may not be completely happy with this background proposition, then you will have to explore more in depth the PowderX possibilities about background. Let us decide that, for a peak position extraction, this background is OK. So, click on OK and it will be subtracted.
Then you have to click on the "alpha-2 strip button", if your powder pattern needs it :
Change the 49% if you are sure about another value (here 53%) and click on "test", and have a look at much details by the zoom option if you need :
This seems OK (more options are available, this is the standard one), so that click on "Finish" and the alpha-2 component will be removed. Then click on the peak search button and on "show". Markers will appear where peaks have been located :
If you are unhappy with the PowderX propositions, then you may play with the 3 parameters ("Select Points", Derivative Limit" and "Intensity Limit") up to fulfill your desires.
If you are happy, click on "OK". A box appears in which you may change the radiation and Wavelength, if appropriate :
For instance, you may believe that 1.54056 is more correct than 1.540598, that is your choice. Then, click on OK, and a box will be opened and proposes a name (nist1976.txt in this case) for saving the extraction results :
You may change the name or not. That .txt file contains your peak positions :
The complete file is below. Care to not confuse
residues of alpha-2 corrections with real peaks :
2Theta d (A) Height Area FWHM 25,574 3,48029 5993,5 58566,4 0,1000 35,139 2,55179 18874,0 145082,7 0,0900 35,303 2,54026 374,2 3248,8 0,0900 37,767 2,38003 2469,4 20254,8 0,0900 41,666 2,16587 576,2 4915,4 0,0900 43,346 2,08573 8803,4 74545,1 0,0900 52,538 1,74040 3979,9 35662,6 0,0900 57,484 1,60186 13317,6 117690,5 0,0900 61,283 1,51134 2370,5 23440,4 0,1000 66,499 1,40489 2307,9 23039,4 0,1000 68,191 1,37410 2518,7 25172,9 0,1000 74,275 1,27587 237,7 2276,7 0,1000 76,846 1,23946 4965,6 42968,4 0,0900 77,209 1,23454 1549,5 15483,1 0,1000 80,676 1,18999 258,3 2231,7 0,0900 84,329 1,14751 229,7 2294,5 0,1000 86,470 1,12451 245,7 2211,5 0,0900 88,963 1,09933 1153,7 11452,0 0,1000 90,677 1,08296 596,0 6376,5 0,1100 91,155 1,07852 382,1 3784,7 0,1000 95,217 1,04296 880,7 8781,4 0,1000 101,039 0,99798 1374,2 13728,0 0,1000 110,951 0,93494 228,9 2514,3 0,1100 116,060 0,90800 392,1 4312,2 0,1100 116,560 0,90555 968,5 10037,9 0,1100 117,816 0,89950 199,4 2127,4 0,1100 127,640 0,85834 808,1 11313,6 0,1400 129,839 0,85047 474,3 6338,6 0,1400 131,032 0,84639 811,5 11144,8 0,1400 136,023 0,83071 668,9 9804,3 0,1500 142,241 0,81408 430,8 6905,6 0,1700 145,119 0,80740 405,0 6802,5 0,1800Best wishes !